View & Download CD data for CD0006412000

Beta-b1 C-terminus (beta b1 subunit of skeletal muscle calcium channel 3.2)


Citation: Andrew J. Miles, Elliot D. Drew, R.W. Janes, B.A. Wallace 2022


Citation: The PCDDB (protein circular dichroism data bank): A bioinformatics resource for protein characterisations and methods development.
Ramalli SG, Miles AJ, Janes RW, Wallace BA., J Mol Biol (2022)


CSA/ACS Standard Spectrum DRS_units Download
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Raw Sample Spectra Download
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Raw Baseline Spectra Download
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Average Sample Download
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Averaged Baseline Download
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HT / High Voltage / Dynode Spectra HT/Dynode Units Download
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Net Smoothed Spectrum Download
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Final Processed Spectrum Delta_Epsilon Download
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Validation report compiled by Validichro v1.4.0.1, 2023-07-31 10:28:08. - FLAG (incomplete)

At a glance
Downloads 704
Depositor Andrew Miles
Uniprot ??
Alpha Fold
PDB
EC
CATH Class
Protein Type intrinsically_disordered

Sample

Protein Name Beta-b1 C-terminus ?
Alternative Protein Names beta B1 subunit of skeletal muscle calcium channel 3.2 ?
Source Organism rat ?
Protein Supplier Dr. N. Berrow (A. Dolphin Lab, University College London) ?
Expression System or natural source E.coli ?
Expressed As CT 6his + 1-94 ?
Mutation Details No data provided ?
Expression tags (if any) No data provided ?
Ligands Present and Concentration or ratio No data provided ?
Macromolecular Partner(s) and Concentration or ratio No data provided ?
Deposition Date 2022-06-21 ?

Experiment

CD or SRCD SRCD ?
Protein Concentration (mg/ml) 3.25 ?
Concentration Quantification Method A280 or A280-denatured ?
Protein Purity (%) No data provided ?
Purity Quantification Method No data provided ?
Buffer Contents and Concentrations 20mM phosphate pH 7.0 ?
Baseline Contents 20mM phosphate pH 7.0 ?
Experimental Temperature (C) 4 ?
Instrument or beamline Daresbury 12.1 ?
Detector Angle (Scattering Angle) No data provided ?
Sample Cell Pathlength (cm) 0.0015 ?
Cell Pathlength Calibration Method Interferometry ?
Sample Cell Type Cylindrical-Demountable ?
Sample Cell Composition Suprasil ?
Sample Chamber Atmosphere Nitrogen ?
Number of repeat scans 3 ?
Continuous or Stepped scan Stepped ?
Maximum (highest) wavelength, nm 280 ?
Minimum (lowest) wavelength, nm 168 ?
Criteria for low wavelength cutoff HT value ?
Wavelength interval, nm 1 ?
Dwell or Averaging time, seconds 1 ?
Experimental Collection date 2004-02-19 ?
Local Spectrum Identifier r8476 ?

Calibration

CSA or ACS CSA ?
Dichroism Units for CSA Standard DRS_units ?
Final Spectrum Calibrated YES ?
CSA/ACS Standard Concentration (mg/ml) 11.8 ?
CSA/ACS Pathlength (mm) 0.101 ?
CSA/ACS Zeroed at No data provided ?
CSA/ACS Date Measured 2022-06-26 ?
CSA/ACS Ratio (192.5nm and 290.0 nm) 2.27 ?
CD signal at 290nm (mdeg) No data provided ?
CSA/ACS Experiment temperature, C 25 ?

Data process.

Molecular Weight 11300 ?
Number of Residues 100 ?
Mean Residue Weight 114.1 ?
Data Processing Software Name CDTool ?
Data Processing Software Version 1.4 ?
Wavelength Range for Zeroing 263-267 ?
Number of Smoothing Points 7 ?

Sec. struct.

Secondary Structure Calculated from AlphaFold2 ?
DSSP value: alpha helix 0.220 ?
DSSP value: 3-10 helix 0.010 ?
DSSP value: pi helix No data provided ?
DSSP value: beta strand No data provided ?
DSSP value: beta bridge No data provided ?
DSSP value: bonded turn 0.014 ?
DSSP value: bend 0.044 ?
DSSP value: loop or irregular 0.716 ?

Tertiary

PDB ID No data provided ?
UniProt ID ?? ?
Enzyme Classification (EC) No data provided ?
Medline Entry No data provided ?
Cath Classification No data provided ?
Sequence HHHHHHMVQK SGMSRGPYPP SQEIPMEVFD PSPQGKYSKR KGRFKRSDGS TSSDTTSNSF VRQGSAESYT SRPSDSDVSL EEDREALRKE AERQALAQLE ?
Type of protein intrinsically_disordered ?
Keyword/phrase A IDP175 test ?
Keyword/phrase B No data provided ?
Keyword/phrase C No data provided ?
Keyword/phrase D No data provided ?
Keyword/phrase E No data provided ?
Keyword/phrase F No data provided ?
Keyword/phrase G No data provided ?
Keyword/phrase H No data provided ?
Keyword/phrase I No data provided ?
Keyword/phrase J No data provided ?
Publication Authors Andrew J. Miles, Elliot D. Drew, R.W. Janes, B.A. Wallace ?
Publication Year 2022 ?
Publication Journal No data provided ?
Publication Title DichroIDP: A Novel Method for Analyses of Intrinsically Disordered Proteins by Circular Dichroism Spectroscopy ?
Publication Volume No data provided ?
Publication Pages No data provided ?

Depositor

Depositor Name Andrew Miles ?
Department/School name crystallography ?
University/Institution/Corporation Birkbeck ?
Depositor Country United Kingdom ?
Name of Principal Investigator (if not depositor) B. A. Wallace ?

Validation report compiled by Validichro v1.4.0.1, 2023-07-31 10:28:08. - FLAG (incomplete)

Depositors Notes:

Missing Wavelengths PASS ?
Maximum Delta Epsilon PASS ?
Minimal Level of Maximum Delta Epsilon PASS ?
Peak Locations PASS ?
Feature Width PASS ?
Experimental Temperature PASS ?
UniProt sequence ?
Molecular Weight PASS ?
Number of Residues PASS ?
Mean Residue Weight value PASS ?
Concentration and Pathlength PASS ?
CSA / ACS peak ratio FLAG ?
CSA / ACS Temperature PASS ?
Peak Shift test PASS ?
Standard Deviation INSUFFICIENT DATA ?
Noise: 260-270nm PASS ?
Flat topped peaks PASS ?
Wavelength range PASS ?
Interval resolution PASS ?
High Tension Voltage 240-260nm INSUFFICIENT DATA ?
Projection Test PASS ?
Standard Deviation At Peak INSUFFICIENT DATA ?
Depositor Note ?

The PCDDB is a development of the Department of Biological Sciences, Institute of Structural and Molecular Biology, Birkbeck College, University of London and the School of Biological and Chemical Sciences, Queen Mary University of London, UK. It is supported by a grant from the BBSRC. Copyright of the design and implementation of this site are retained by the schools and the authors.