View & Download CD data for CD0004553000

Poly-proline II Native (poly-l-proline)


Citation: Jose L.S. Lopes, Andrew J. Miles, Lee Whitmore, B.A. Wallace 2014 Protein Science 23 1765-1772


Citation: The PCDDB (protein circular dichroism data bank): A bioinformatics resource for protein characterisations and methods development.
Ramalli SG, Miles AJ, Janes RW, Wallace BA., J Mol Biol (2022)


CSA/ACS Standard Spectrum Millidegrees (theta) Download
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HT / High Voltage / Dynode Spectra HT/Dynode Units Download
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Final Processed Spectrum Delta Epsilon Download
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Validation report compiled by Validichro v1.3.0, 2014-12-17, 4:46pm. - FLAG (Incomplete)

At a glance
Downloads 819
Depositor Jose Lopes
Uniprot
Alpha Fold
PDB
EC
CATH Class
Protein Type soluble fibrous

Sample

Protein Name poly-proline II native ?
Alternative Protein Names Poly-L-proline ?
Source Organism synthetic ?
Protein Supplier Sigma-Aldrich ?
Expression System or natural source homopolymer ?
Expressed As homopolymer ?
Mutation Details No data provided ?
Expression tags (if any) No data provided ?
Ligands Present and Concentration or ratio no ligands ?
Macromolecular Partner(s) and Concentration or ratio no partner ?
Deposition Date 2014-12-19 ?

Experiment

CD or SRCD SRCD ?
Protein Concentration (mg/ml) 2.4 ?
Concentration Quantification Method Supplier value ?
Protein Purity (%) No data provided ?
Purity Quantification Method No data provided ?
Buffer Contents and Concentrations 10 mM sodium phosphate (pH 7.0) ?
Baseline Contents 10 mM sodium phosphate (pH 7.0) ?
Experimental Temperature (C) 25 ?
Instrument or beamline ISA CD1 ?
Detector Angle (Scattering Angle) No data provided ?
Sample Cell Pathlength (cm) 0.0015 ?
Cell Pathlength Calibration Method Interferometry ?
Sample Cell Type Cylindrical-Demountable ?
Sample Cell Composition Quartz ?
Sample Chamber Atmosphere Nitrogen ?
Number of repeat scans 3 ?
Continuous or Stepped scan Stepped ?
Maximum (highest) wavelength, nm 280 ?
Minimum (lowest) wavelength, nm 165 ?
Criteria for low wavelength cutoff HT value ?
Wavelength interval, nm 1 ?
Dwell or Averaging time, seconds No data provided ?
Experimental Collection date 2013-01-14 ?
Local Spectrum Identifier a32364 ?

Calibration

CSA or ACS CSA ?
Dichroism Units for CSA Standard Millidegrees (theta) ?
Final Spectrum Calibrated YES ?
CSA/ACS Standard Concentration (mg/ml) No data provided ?
CSA/ACS Pathlength (mm) No data provided ?
CSA/ACS Zeroed at 230-235 ?
CSA/ACS Date Measured 2013-01-14 ?
CSA/ACS Ratio (192.5nm and 290.0 nm) No data provided ?
CD signal at 290nm (mdeg) No data provided ?
CSA/ACS Experiment temperature, C 25 ?

Data process.

Molecular Weight 9729.6 ?
Number of Residues 100 ?
Mean Residue Weight 98.3 ?
Data Processing Software Name CDTool ?
Data Processing Software Version No data provided ?
Wavelength Range for Zeroing 263-270 ?
Number of Smoothing Points 7 ?

Sec. struct.

Secondary Structure Calculated from No data provided ?
DSSP value: alpha helix No data provided ?
DSSP value: 3-10 helix No data provided ?
DSSP value: pi helix No data provided ?
DSSP value: beta strand No data provided ?
DSSP value: beta bridge No data provided ?
DSSP value: bonded turn No data provided ?
DSSP value: bend No data provided ?
DSSP value: loop or irregular No data provided ?

Tertiary

PDB ID No data provided ?
UniProt ID No data provided ?
Enzyme Classification (EC) No data provided ?
Medline Entry No data provided ?
Cath Classification No data provided ?
Sequence PPPPPPPPPP PPPPPPPPPP PPPPPPPPPP PPPPPPPPPP PPPPPPPPPP PPPPPPPPPP PPPPPPPPPP PPPPPPPPPP PPPPPPPPPP PPPPPPPPPP ?
Type of protein soluble fibrous ?
Keyword/phrase A Poly-L-proline (MW 1,000-10,000, Sigma-Aldrich) ?
Keyword/phrase B homopolymer ?
Keyword/phrase C No data provided ?
Keyword/phrase D No data provided ?
Keyword/phrase E No data provided ?
Keyword/phrase F No data provided ?
Keyword/phrase G No data provided ?
Keyword/phrase H No data provided ?
Keyword/phrase I No data provided ?
Keyword/phrase J No data provided ?
Publication Authors Jose L.S. Lopes, Andrew J. Miles, Lee Whitmore, B.A. Wallace ?
Publication Year 2014 ?
Publication Journal Protein Science ?
Publication Title Distinct circular dichroism spectroscopic signatures of polyproline II and unordered secondary structures: Applications in secondary structure analyses. ?
Publication Volume 23 ?
Publication Pages 1765-1772 ?

Depositor

Depositor Name Jose Lopes ?
Department/School name Crystallography ?
University/Institution/Corporation Birkbeck College ?
Depositor Country U.K. ?
Name of Principal Investigator (if not depositor) BA Wallace ?

Validation report compiled by Validichro v1.3.0, 2014-12-17, 4:46pm. - FLAG (Incomplete)

Depositors Notes: Poly-proline used presents molecular weight (MW) from 1,000-10,000. For the deposited file, authors have used the MW of a polypeptide that would be 100 prolines long (9729.6), number of residues as 100, MRW of 98.3, and a sequence of 100 proline residues

Missing Wavelengths PASS ?
Maximum Delta Epsilon PASS ?
Minimal Level of Maximum Delta Epsilon PASS ?
Peak Locations PASS ?
Feature Width PASS ?
Experimental Temperature PASS ?
UniProt sequence FLAG ?
Molecular Weight PASS ?
Number of Residues PASS ?
Mean Residue Weight value PASS ?
Concentration and Pathlength PASS ?
CSA / ACS peak ratio calculation failed ?
CSA / ACS Temperature PASS ?
Peak Shift test PASS ?
Standard Deviation INSUFFICIENT DATA ?
Noise: 260-270nm PASS ?
Flat topped peaks PASS ?
Wavelength range PASS ?
Interval resolution PASS ?
High Tension Voltage 240-260nm INSUFFICIENT DATA ?
Projection Test PASS ?
Standard Deviation At Peak INSUFFICIENT DATA ?
Depositor Note Poly-proline used presents molecular weight (MW) from 1,000-10,000. For the deposited file, authors have used the MW of a polypeptide that would be 100 prolines long (9729.6), number of residues as 100, MRW of 98.3, and a sequence of 100 proline residues ?

The PCDDB is a development of the Department of Biological Sciences, Institute of Structural and Molecular Biology, Birkbeck College, University of London and the School of Biological and Chemical Sciences, Queen Mary University of London, UK. It is supported by a grant from the BBSRC. Copyright of the design and implementation of this site are retained by the schools and the authors.