View & Download CD data for CD0003897000

Human DUTPase (dutp pyrophosphatase)


Citation: No citation information currently associated with this entry.


Citation: The PCDDB (protein circular dichroism data bank): A bioinformatics resource for protein characterisations and methods development.
Ramalli SG, Miles AJ, Janes RW, Wallace BA., J Mol Biol (2022)


CSA/ACS Standard Spectrum Millidegrees (theta) Download
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Raw Sample Spectra Millidegrees (theta) Download
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Raw Sample Spectra 2 Millidegrees (theta) Download
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Raw Sample Spectra 3 Millidegrees (theta) Download
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Raw Sample Spectra 4 Millidegrees (theta) Download
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Raw Sample Spectra 5 Millidegrees (theta) Download
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Raw Sample Spectra 6 Millidegrees (theta) Download
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Raw Baseline Spectra Millidegrees (theta) Download
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Raw Baseline Spectra 2 Millidegrees (theta) Download
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Raw Baseline Spectra 3 Millidegrees (theta) Download
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Average Sample Millidegrees (theta) Download
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Averaged Baseline Millidegrees (theta) Download
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HT / High Voltage / Dynode Spectra HT/Dynode Units Download
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HT / High Voltage / Dynode Spectra 2 HT/Dynode Units Download
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HT / High Voltage / Dynode Spectra 3 HT/Dynode Units Download
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HT / High Voltage / Dynode Spectra 4 HT/Dynode Units Download
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HT / High Voltage / Dynode Spectra 5 HT/Dynode Units Download
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HT / High Voltage / Dynode Spectra 6 HT/Dynode Units Download
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Net Smoothed Spectrum Millidegrees (theta) Download
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Final Processed Spectrum Delta Epsilon Download
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Validation report compiled by Validichro v1.4.0, 2015-04-01, 3:55pm. - FLAG

At a glance
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Depositor Frank Wien
Uniprot P33316
Alpha Fold
PDB 1Q5U
EC 3.6.1.23
CATH Class 2.70.40.10
Protein Type soluble globular

Sample

Protein Name human dUTPase ?
Alternative Protein Names dUTP pyrophosphatase ?
Source Organism Homo sapiens ?
Protein Supplier Beta Vrtessy, Institute of Enzymology, Hung. Acad. Sci. ?
Expression System or natural source E. coli ?
Expressed As Wild-type ?
Mutation Details Homo sapiens. Human. Organism_taxid: 9606. Gene: hdut. Expressed in: escherichia coli bl21(de3). Expression_system_taxid: 469008 ?
Expression tags (if any) N,HHHHHH ?
Ligands Present and Concentration or ratio No data provided ?
Macromolecular Partner(s) and Concentration or ratio No data provided ?
Deposition Date 2015-04-01 ?

Experiment

CD or SRCD SRCD ?
Protein Concentration (mg/ml) 3.3 ?
Concentration Quantification Method QAA ?
Protein Purity (%) >95% ?
Purity Quantification Method SDS gels ?
Buffer Contents and Concentrations 10mM Phophate buffer pH 7.5 ?
Baseline Contents dialysate ?
Experimental Temperature (C) 20 ?
Instrument or beamline Soleil DISCO ?
Detector Angle (Scattering Angle) 60 ?
Sample Cell Pathlength (cm) 0.0024 ?
Cell Pathlength Calibration Method Interferometry ?
Sample Cell Type Cylindrical-Demountable ?
Sample Cell Composition CaF2 ?
Sample Chamber Atmosphere Nitrogen ?
Number of repeat scans 6 ?
Continuous or Stepped scan Stepped ?
Maximum (highest) wavelength, nm 271 ?
Minimum (lowest) wavelength, nm 175 ?
Criteria for low wavelength cutoff HT value ?
Wavelength interval, nm 1 ?
Dwell or Averaging time, seconds 1.2 ?
Experimental Collection date 2012-04-04 ?
Local Spectrum Identifier paprika7 ?

Calibration

CSA or ACS CSA ?
Dichroism Units for CSA Standard Millidegrees (theta) ?
Final Spectrum Calibrated YES ?
CSA/ACS Standard Concentration (mg/ml) 6.3 ?
CSA/ACS Pathlength (mm) 0.1 ?
CSA/ACS Zeroed at 230-245 ?
CSA/ACS Date Measured 2012-04-04 ?
CSA/ACS Ratio (192.5nm and 290.0 nm) 1.95 ?
CD signal at 290nm (mdeg) 23.9 ?
CSA/ACS Experiment temperature, C 25 ?

Data process.

Molecular Weight 16218.2 ?
Number of Residues 147 ?
Mean Residue Weight 111.08 ?
Data Processing Software Name CDTool ?
Data Processing Software Version latest ?
Wavelength Range for Zeroing 263-267 ?
Number of Smoothing Points 7 ?

Sec. struct.

Secondary Structure Calculated from 1Q5U.pdb ?
DSSP value: alpha helix 0.48 ?
DSSP value: 3-10 helix 0.0 ?
DSSP value: pi helix 0.0 ?
DSSP value: beta strand 0.385 ?
DSSP value: beta bridge 0.014 ?
DSSP value: bonded turn 0.086 ?
DSSP value: bend 0.088 ?
DSSP value: loop or irregular 0.379 ?

Tertiary

PDB ID 1Q5U ?
UniProt ID P33316 ?
Enzyme Classification (EC) 3.6.1.23 ?
Medline Entry No data provided ?
Cath Classification 2.70.40.10 ?
Sequence HHHHHHMQLR FARLSEHATA PTRGSARAAG YDLYSAYDYT IPPMEKAVVK TDIQIALPSG CYGRVAPRSG LAAKHFIDVG AGVIDEDYRG NVGVVLFNFG KEKFEVKKGD RIAQLICERI FYPEIEEVQA LDDTERGSGG FGSTGKN ?
Type of protein soluble globular ?
Keyword/phrase A Human dutp pyrophosphatase ?
Keyword/phrase B No data provided ?
Keyword/phrase C No data provided ?
Keyword/phrase D No data provided ?
Keyword/phrase E No data provided ?
Keyword/phrase F No data provided ?
Keyword/phrase G No data provided ?
Keyword/phrase H No data provided ?
Keyword/phrase I No data provided ?
Keyword/phrase J No data provided ?
Publication Authors No data provided ?
Publication Year No data provided ?
Publication Journal No data provided ?
Publication Title No data provided ?
Publication Volume No data provided ?
Publication Pages No data provided ?

Depositor

Depositor Name Frank Wien ?
Department/School name Experiences ?
University/Institution/Corporation SOLEIL Synchrotron ?
Depositor Country France ?
Name of Principal Investigator (if not depositor) József Kardos ?

Validation report compiled by Validichro v1.4.0, 2015-04-01, 3:55pm. - FLAG

Depositors Notes: Uniprot sequence does not match the protein sequence used because it is a cloned protein identical to the pdb structure. It does not contain the mitochondrial signal sequence, this is the 112-252 residues fragment of the Uniprot sequence. Standard deviation was not subject to a Flag using Validichro instead this protein demonstrates a flag for max magnitude. We suggest: the spectrum under analysis is perfectly valid, but novel and be worth inclusion in the reference set.

Missing Wavelengths PASS ?
Maximum Delta Epsilon PASS ?
Minimal Level of Maximum Delta Epsilon PASS ?
Peak Locations PASS ?
Feature Width PASS ?
Experimental Temperature PASS ?
UniProt sequence FLAG ?
Molecular Weight PASS ?
Number of Residues PASS ?
Mean Residue Weight value PASS ?
Concentration and Pathlength PASS ?
CSA / ACS peak ratio PASS ?
CSA / ACS Temperature PASS ?
Peak Shift test PASS ?
Standard Deviation FLAG ?
Noise: 260-270nm PASS ?
Flat topped peaks PASS ?
Wavelength range PASS ?
Interval resolution PASS ?
High Tension Voltage 240-260nm PASS ?
Projection Test PASS ?
Standard Deviation At Peak PASS ?
Depositor Note Uniprot sequence does not match the protein sequence used because it is a cloned protein identical to the pdb structure. It does not contain the mitochondrial signal sequence, this is the 112-252 residues fragment of the Uniprot sequence. Standard deviation was not subject to a Flag using Validichro instead this protein demonstrates a flag for max magnitude. We suggest: the spectrum under analysis is perfectly valid, but novel and be worth inclusion in the reference set. ?

The PCDDB is a development of the Department of Biological Sciences, Institute of Structural and Molecular Biology, Birkbeck College, University of London and the School of Biological and Chemical Sciences, Queen Mary University of London, UK. It is supported by a grant from the BBSRC. Copyright of the design and implementation of this site are retained by the schools and the authors.