View & Download CD data for CD0000063100

Ribonuclease Pancreatic (rnase1, rns1)


Citation: Miles, A.J., Whitmore, L., Janes, R.W. & Wallace, B.A. 2014 Scientific data


Citation: The PCDDB (protein circular dichroism data bank): A bioinformatics resource for protein characterisations and methods development.
Ramalli SG, Miles AJ, Janes RW, Wallace BA., J Mol Biol (2022)


CSA/ACS Standard Spectrum Millidegrees \(theta\) Download
View Plot
Raw Sample Spectra Millidegrees (theta) Download
View Plot
Raw Sample Spectra 2 Millidegrees (theta) Download
View Plot
Raw Sample Spectra 3 Millidegrees (theta) Download
View Plot
Raw Baseline Spectra Millidegrees (theta) Download
View Plot
Raw Baseline Spectra 2 Millidegrees (theta) Download
View Plot
Raw Baseline Spectra 3 Millidegrees (theta) Download
View Plot
Average Sample Millidegrees (theta) Download
View Plot
Averaged Baseline Millidegrees (theta) Download
View Plot
HT / High Voltage / Dynode Spectra HT/Dynode Units Download
View Plot
HT / High Voltage / Dynode Spectra 2 HT/Dynode Units Download
View Plot
HT / High Voltage / Dynode Spectra 3 HT/Dynode Units Download
View Plot
Net Smoothed Spectrum Millidegrees (theta) Download
View Plot
Final Processed Spectrum Delta Epsilon Download
View Plot

Validation report compiled by Validichro v1.4.0.1, 2022-09-20 10:59:15. - PASS

At a glance
Downloads 1834
Depositor Andrew Miles
Uniprot P61823
Alpha Fold
PDB 3rn3
EC 3.1.27.5
CATH Class 3.10.130.10
Protein Type soluble globular

Sample

Protein Name Ribonuclease pancreatic ?
Alternative Protein Names RNASE1, RNS1 ?
Source Organism Bos taurus ?
Protein Supplier Calbiochem ?
Expression System or natural source natural source ?
Expressed As Wild-type ?
Mutation Details No data provided ?
Expression tags (if any) No data provided ?
Ligands Present and Concentration or ratio No data provided ?
Macromolecular Partner(s) and Concentration or ratio No data provided ?
Deposition Date 2014-03-26 ?

Experiment

CD or SRCD SRCD ?
Protein Concentration (mg/ml) 7.50 ?
Concentration Quantification Method Nanodrop ?
Protein Purity (%) >95 ?
Purity Quantification Method SDS gels ?
Buffer Contents and Concentrations H2O ?
Baseline Contents H2O ?
Experimental Temperature (C) 4 ?
Instrument or beamline ISA UV1 ?
Detector Angle (Scattering Angle) No data provided ?
Sample Cell Pathlength (cm) 0.0015 ?
Cell Pathlength Calibration Method Interferometry ?
Sample Cell Type Rectangular-Demountable ?
Sample Cell Composition Suprasil ?
Sample Chamber Atmosphere Nitrogen ?
Number of repeat scans 3 ?
Continuous or Stepped scan Stepped ?
Maximum (highest) wavelength, nm 280 ?
Minimum (lowest) wavelength, nm 175 ?
Criteria for low wavelength cutoff HT value ?
Wavelength interval, nm 1 ?
Dwell or Averaging time, seconds 2 ?
Experimental Collection date 2005-02-25 ?
Local Spectrum Identifier aa2887 ?

Calibration

CSA or ACS CSA ?
Dichroism Units for CSA Standard Millidegrees \(theta\) ?
Final Spectrum Calibrated YES ?
CSA/ACS Standard Concentration (mg/ml) 9.42 ?
CSA/ACS Pathlength (mm) 0.1 ?
CSA/ACS Zeroed at 235-240 ?
CSA/ACS Date Measured 2005-02-25 ?
CSA/ACS Ratio (192.5nm and 290.0 nm) 1.87 ?
CD signal at 290nm (mdeg) 31.40 ?
CSA/ACS Experiment temperature, C 25 ?

Data process.

Molecular Weight 13690 ?
Number of Residues 124 ?
Mean Residue Weight 111.3 ?
Data Processing Software Name CDTool ?
Data Processing Software Version 1.4 ?
Wavelength Range for Zeroing 263-270 ?
Number of Smoothing Points 7 ?

Sec. struct.

Secondary Structure Calculated from PDB file ?
DSSP value: alpha helix 0.177 ?
DSSP value: 3-10 helix 0.032 ?
DSSP value: pi helix 0.000 ?
DSSP value: beta strand 0.331 ?
DSSP value: beta bridge 0.024 ?
DSSP value: bonded turn 0.145 ?
DSSP value: bend 0.105 ?
DSSP value: loop or irregular 0.185 ?

Tertiary

PDB ID 3rn3 ?
UniProt ID P61823 ?
Enzyme Classification (EC) 3.1.27.5 ?
Medline Entry No data provided ?
Cath Classification 3.10.130.10 ?
Sequence KETAAAKFER QHMDSSTSAA SSSNYCNQMM KSRNLTKDRC KPVNTFVHES LADVQAVCSQ KNVACKNGQT NCYQSYSTMS ITDCRETGSS KYPNCAYKTT QANKHIIVAC EGNPYVPVHF DASV ?
Type of protein soluble globular ?
Keyword/phrase A SP175a ?
Keyword/phrase B single domain type ?
Keyword/phrase C mixed alpha beta ?
Keyword/phrase D No data provided ?
Keyword/phrase E No data provided ?
Keyword/phrase F No data provided ?
Keyword/phrase G No data provided ?
Keyword/phrase H No data provided ?
Keyword/phrase I No data provided ?
Keyword/phrase J No data provided ?
Publication Authors Miles, A.J., Whitmore, L., Janes, R.W. & Wallace, B.A. ?
Publication Year 2014 ?
Publication Journal Scientific data ?
Publication Title A "Gold Standard" Reference Dataset for Protein Circular Dichroism Spectral and Meta-Data ?
Publication Volume No data provided ?
Publication Pages No data provided ?

Depositor

Depositor Name Andrew Miles ?
Department/School name crystallography ?
University/Institution/Corporation Birkbeck ?
Depositor Country United Kingdom ?
Name of Principal Investigator (if not depositor) B.A. Wallace ?

Validation report compiled by Validichro v1.4.0.1, 2022-09-20 10:59:15. - PASS

Depositors Notes:

Missing Wavelengths PASS ?
Maximum Delta Epsilon PASS ?
Minimal Level of Maximum Delta Epsilon PASS ?
Peak Locations PASS ?
Feature Width PASS ?
Experimental Temperature PASS ?
UniProt sequence ?
Molecular Weight PASS ?
Number of Residues PASS ?
Mean Residue Weight value PASS ?
Concentration and Pathlength PASS ?
CSA / ACS peak ratio PASS ?
CSA / ACS Temperature PASS ?
Peak Shift test PASS ?
Standard Deviation PASS ?
Noise: 260-270nm PASS ?
Flat topped peaks PASS ?
Wavelength range PASS ?
Interval resolution PASS ?
High Tension Voltage 240-260nm PASS ?
Projection Test PASS ?
Standard Deviation At Peak PASS ?
Depositor Note ?

The PCDDB is a development of the Department of Biological Sciences, Institute of Structural and Molecular Biology, Birkbeck College, University of London and the School of Biological and Chemical Sciences, Queen Mary University of London, UK. It is supported by a grant from the BBSRC. Copyright of the design and implementation of this site are retained by the schools and the authors.